SAMPLE PREP./SIZE PYROL. CONDITIONS TOTAL ION COUNTS
TEICHOIC ACID (from Bacillus svbtiUs)
poly[2,3-glycerol-phosphate] with DGlcg-units linked to position 1 of glycerol; see insert in spectrum gift from Dr. J.T.M. Wouters, Lab. of Microbiology, Univ.
of Amsterdam, The Netherlands suspension in methanol; 10 yg standard
REMARKS - Sample prepared following ref. 172. The terminal side chain glucose units appear to give rise to peaks at m/z 96, 98, 110 and 126 (see Spectra A.1-A.4), whereas the most pronounced fragments from the glycerol moieties are thought to be m/z 61 (probably an EI fragment) and m/z 44. Peaks at m/z 36, 38 (HC1+") indicate the presence of chloride in the sample.
in 2 uj
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